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Tetrahedron Letters. 2003 Feb 24;44:1831-3
Microwave oven synthesis of esters promoted by imidazole.
Hirose T, Kopek BG, Wang Z, Yusa R, Baldwin BW
Note: Research in this publication was not performed at Janelia.
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Abstract
Using imidazole as promotion agent, primary, secondary and phenolic alcohol compounds were esterified with aliphatic and aromatic carboxylic acid anhydrides. Heating a ternary mixture of alcohol, anhydride and imidazole in an unmodified microwave oven produced esters in low to high yields, depending on the steric bulk of the alcohol.
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