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02/24/03 |
Microwave oven synthesis of esters promoted by imidazole.
Tetrahedron Letters. 2003 Feb 24;44:1831-3
Using imidazole as promotion agent, primary, secondary and phenolic alcohol compounds were esterified with aliphatic and aromatic carboxylic acid anhydrides. Heating a ternary mixture of alcohol, anhydride and imidazole in an unmodified microwave oven produced esters in low to high yields, depending on the steric bulk of the alcohol.